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Enhancing Interfacial Bonding and Pore Structure Optimization in 3D-Printed High-Strength ECC with Steel-PE Hybrid Fibers (2025-06)

10.1016/j.cscm.2025.e04934

Zhao Yu, Shen Guanghai, Zhu Lingli, Ding Yahong,  Guan Xuemao
Journal Article - Case Studies in Construction Materials, Vol. 23, No. e04934

Abstract

Engineered cementitious composites (ECC) are ideal candidates for 3D-printed concrete (3DPC) due to their excellent strain-hardening properties; however, the interlayer interfacial defects caused by the layer-by-layer stacking process severely restrict the development of their mechanical properties. In this study, we propose to adopt a steel fiber/polyethylene(PE) fiber hybrid reinforcement strategy to systematically investigate the mechanism of the influence of steel fiber compounding ratio (0–0.6 vol%) on the splitting strength and pore structure of the interlayer interfaces of 3D-printed high-strength ECC (HS-ECC). The three-dimensional distribution of pores was quantitatively resolved by X-ray computed tomography (X-CT), and the micro-morphology of the transition zone at the fiber-matrix interface was observed by scanning electron microscopy (SEM). The test shows that: when the steel fiber doping is increased to 0.6 %, the compressive strength is improved by about 15 %, and the interfacial splitting tensile strength is improved by 50.12 %, but the uniaxial tensile strain capacity decreases by 18.92 %, which reveals that there is a strength-ductility trade-off effect in the proportion of fiber mixing; the X-CT reconstruction reveals that the porosity within the strips of the printed specimen is reduced by 15.01 % compared with that of the poured molding and the porosity is dominated by small pores of a pore size of < 100 μm, but the interlayer interfacial interface microforms. The X-CT and SEM analyses confirmed that the steel fibers showed a significant orientation distribution in the printing direction, which inhibited the interface crack extension through the bridging effect. By optimizing the fiber orientation distribution and the microstructure of the interlayer interface, the compound-mixed steel fibers significantly improved the interfacial splitting tensile strength, which provides an effective way to solve the problem of weak interlayer surfaces in 3DPC, and is of great significance in improving the quality of 3DPC.

25 References

  1. Al-Qutaifi Sarah, Nazari Ali, Bagheri Ali (2018-07)
    Mechanical Properties of Layered Geopolymer Structures Applicable in Concrete 3D Printing
  2. Arunothayan Arun, Nematollahi Behzad, Ranade Ravi, Bong Shin et al. (2021-02)
    Fiber-Orientation Effects on Ultra-High-Performance Concrete Formed by 3D Printing
  3. Bai Meiyan, Xiao Jianzhuang, Ding Tao, Yu Kequan (2024-12)
    Interfacial Bond-Properties Between 3D Printed Engineered Cementitious Composite and Post-Cast Concrete
  4. Buswell Richard, Silva Wilson, Jones Scott, Dirrenberger Justin (2018-06)
    3D Printing Using Concrete-Extrusion:
    A Roadmap for Research
  5. Chen Yu, Çopuroğlu Oğuzhan, Rodríguez Claudia, Filho Fernando et al. (2021-02)
    Characterization of Air-Void Systems in 3D Printed Cementitious Materials Using Optical Image Scanning and X-Ray Computed Tomography
  6. Ding Tao, Xiao Jianzhuang, Mechtcherine Viktor (2023-05)
    Microstructure and Mechanical Properties of Inter-Layer Regions in Extrusion-Based 3D Printed Concrete:
    A Critical Review
  7. Heever Marchant, Plessis Anton, Kruger Jacques, Zijl Gideon (2022-01)
    Evaluating the Effects of Porosity on the Mechanical Properties of Extrusion-Based 3D Printed Concrete
  8. Heras Murica Daniel, Genedy Moneeb, Taha Mahmoud (2020-09)
    Examining the Significance of Infill-Printing-Pattern on the Anisotropy of 3D Printed Concrete
  9. Kruger Jacques, Plessis Anton, Zijl Gideon (2020-12)
    An Investigation into the Porosity of Extrusion-Based 3D Printed Concrete
  10. Li Victor, Bos Freek, Yu Kequan, McGee Wesley et al. (2020-04)
    On the Emergence of 3D Printable Engineered, Strain-Hardening Cementitious Composites
  11. Moini Mohamadreza, Baghaie Ahmadreza, Rodriguez Fabian, Zavattieri Pablo et al. (2021-06)
    Quantitative Microstructural Investigation of 3D Printed and Cast Cement-Pastes Using Micro-Computed Tomography- and Image-Analysis
  12. Nematollahi Behzad, Vijay Praful, Sanjayan Jay, Nazari Ali et al. (2018-11)
    Effect of Polypropylene Fiber Addition on Properties of Geopolymers Made by 3D Printing for Digital Construction
  13. Ogura Hiroki, Nerella Venkatesh, Mechtcherine Viktor (2018-08)
    Developing and Testing of Strain-Hardening Cement-Based Composites (SHCC) in the Context of 3D Printing
  14. Panda Biranchi, Ruan Shaoqin, Unluer Cise, Tan Ming (2018-11)
    Improving the 3D Printability of High-Volume Fly-Ash Mixtures via the Use of Nano-Attapulgite-Clay
  15. Putten Jolien, Deprez Maxim, Cnudde Veerle, Schutter Geert et al. (2019-09)
    Microstructural Characterization of 3D Printed Cementitious Materials
  16. Sanjayan Jay, Nematollahi Behzad, Xia Ming, Marchment Taylor (2018-04)
    Effect of Surface Moisture on Inter-Layer Strength of 3D Printed Concrete
  17. Wangler Timothy, Lloret-Fritschi Ena, Reiter Lex, Hack Norman et al. (2016-10)
    Digital Concrete:
    Opportunities and Challenges
  18. Wang Li, Yang Yu, Yao Liang, Ma Guowei (2022-02)
    Interfacial Bonding Properties of 3D Printed Permanent Formwork with the Post-Casted Concrete
  19. Wolfs Robert, Bos Freek, Salet Theo (2019-03)
    Hardened Properties of 3D Printed Concrete:
    The Influence of Process Parameters on Inter-Layer Adhesion
  20. Yang Yekai, Wu Chengqing, Liu Zhongxian, Wang Hailiang et al. (2021-10)
    Mechanical Anisotropy of Ultra-High-Performance Fiber-Reinforced Concrete for 3D Printing
  21. Yang Rijiao, Zeng Qiang, Peng Yu, Wang Hailong et al. (2022-05)
    Anomalous Matrix and Inter-Layer Pore-Structure of 3D Printed Fiber-Reinforced Cementitious Composites
  22. Yu Shiwei, Xia Ming, Sanjayan Jay, Yang Lin et al. (2021-07)
    Microstructural Characterization of 3D Printed Concrete
  23. Zareiyan Babak, Khoshnevis Behrokh (2017-08)
    Effects of Interlocking on Inter-Layer Adhesion and Strength of Structures in 3D Printing of Concrete
  24. Zhang Yi, Tao Yaxin, Godinho Jose, Ren Qiang et al. (2024-11)
    Layer Interface Characteristics and Adhesion of 3D Printed Cement-Based Materials Exposed to Post-Printing Temperature Disturbance
  25. Zhou Wen, Zhang Yamei, Ma Lei, Li Victor (2022-04)
    Influence of Printing Parameters on 3D Printing Engineered Cementitious Composites

4 Citations

  1. Zhang Xiaoyue, Chen Zhengren, Zhou Xinting, Li Zheng et al. (2026-01)
    Experimental Investigation on the Mechanical Performance of 3D-Printed Concrete-Glued Laminated Timber Composite Beams
  2. Raza Ali, Tan Binglin, Jiajia Zhou, Umar Muhammad et al. (2025-11)
    Evaluation of Mechanical and Microstructural Properties of Sustainable 3D-Printed Engineered Cementitious Composites Incorporating Hybrid PE/PVA Fibers and Yellow River Sand
  3. Zhang Hui, Wu Jie, Huang Bo-Tao, Yu Rena et al. (2025-11)
    Cross-Scale Mechanisms of Anisotropy in 3D-Printed Ultra-High-Performance Concrete
  4. Chen Wenguang, Yu Jie, Ye Junhong, Yu Jiangtao et al. (2025-11)
    3D Printed High-Performance Fiber-Reinforced Cementitious Composites:
    Fresh, Mechanical, and Microstructural Properties

BibTeX
@article{zhao_shen_zhu_ding.2025.EIBaPSOi3PHSEwSPHF,
  author            = "Yu Zhao and Guanghai Shen and Lingli Zhu and Yahong Ding and Xuemao Guan",
  title             = "Enhancing Interfacial Bonding and Pore Structure Optimization in 3D-Printed High-Strength ECC with Steel-PE Hybrid Fibers",
  doi               = "10.1016/j.cscm.2025.e04934",
  year              = "2025",
  journal           = "Case Studies in Construction Materials",
  volume            = "23",
  pages             = "e04934",
}
Formatted Citation

Y. Zhao, G. Shen, L. Zhu, Y. Ding and X. Guan, “Enhancing Interfacial Bonding and Pore Structure Optimization in 3D-Printed High-Strength ECC with Steel-PE Hybrid Fibers”, Case Studies in Construction Materials, vol. 23, p. e04934, 2025, doi: 10.1016/j.cscm.2025.e04934.

Zhao, Yu, Guanghai Shen, Lingli Zhu, Yahong Ding, and Xuemao Guan. “Enhancing Interfacial Bonding and Pore Structure Optimization in 3D-Printed High-Strength ECC with Steel-PE Hybrid Fibers”. Case Studies in Construction Materials 23 (2025): e04934. https://doi.org/10.1016/j.cscm.2025.e04934.